求高手将我的摘要翻译成英文.1、摘要:探讨了以硅胶为吸附剂,应用柱层析分离青霉噻唑酸的工艺条件.TLC法确定了青霉噻唑酸

求高手将我的摘要翻译成英文.
1、摘要:探讨了以硅胶为吸附剂,应用柱层析分离青霉噻唑酸的工艺条件.TLC法确定了青霉噻唑酸的薄层层析展开剂为乙酸乙酯:丙酮:乙酸(5:2:0.1).通过对洗脱方式、洗脱流速和上样量的考察,确定了柱层析的最佳工艺条件:乙酸乙酯、丙酮梯度洗脱,上样量1.0%,流速为1.0mL/min.最后经高效液相分析,产品中青霉噻唑酸的纯度可达90%.
2、关键词:青霉噻唑酸;硅胶柱层析;分离纯化
3、 恒定配比洗脱的TLC检测结果 梯度洗脱的TLC检测结果
4、纯化后的青霉噻唑酸TLC谱图 纯化后的青霉噻唑酸HPLC谱图
拒绝所有 2024-07-26 悬赏10金币 已收到2个回答

u3342391

共回答了185个问题采纳率:87%

1,the author discusses:for adsorbent,application of silica gel column chromatography separation penicillium Margaret acid technology conditions.TLC method is used to determine the Margaret penicillium acid on the thin layer chromatography agent for ethyl acetate:acetone:acetic acid (5:2:0.1).Through to the elution way,with the flow velocity and the investigation of the sample weight,and the column chromatography,the optimum process conditions of ethyl acetate,acetone gradient elution and sample weight,velocity on 1.0% for 1.0 mL/min.Finally the highly effective liquid phase analysis,the products covered the purity of Margaret mildew acid can be up to 90%.
2,key words:penicillium acid,Margaret Silica gel column chromatography; purification.
3,a constant ratio of the TLC test results with the gradient itself TLC test results.
4 and purification of the mold after Margaret acid TLC spectra of purified penicillium acid HPLC spectra Margaret.
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tony123

共回答了172个问题

1、摘要:探讨了以硅胶为吸附剂,应用柱层析分离青霉噻唑酸的工艺条件。TLC法确定了青霉噻唑酸的薄层层析展开剂为乙酸乙酯:丙酮:乙酸(5:2:0.1)。通过对洗脱方式、洗脱流速和上样量的考察,确定了柱层析的最佳工艺条件:乙酸乙酯、丙酮梯度洗脱,上样量1.0%,流速为1.0mL/min。最后经高效液相分析,产品中青霉噻唑酸的纯度可达90%。
1, Abstract: the paper dis...
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